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| Mössbauer and Gamma spectrometer
|
| Reference: |
IRCPK/06/TO/11 |
| Organization: |
Cracow University of Technology |
| IRC Name: |
IRC South Poland |
| Country: |
Poland |
| Entry Date: |
Thu, June 28, 2001 |
| Last Update: |
Tue, October 29, 2002 |
| Deadline: |
Fri, October 10, 2003 |
| Abstract:
A Polish SME has developed a computer-controlled Mössbauer/Gamma
spectrometer flexible in design and operation has been fully
developed and tested. Driving software and very sophisticated data
processing software MOSGRAF operating under Microsoft Windows9x
systems have been elaborated. The company is looking for a partner
from the medicine or metrology branch for co-operation. |
| Description:
A complete spectrometer is designed as a set of modules fitting
into the Euro-bin and communicating with the computer via the fast
link. It has the following features: 1. Two multi-scalar data
banks having up to 4096 channels with 32-bit capacity 2. Two
amplitude analyser data banks having up to 4096 channels with 32-bit
capacity 3. Built-in γ-ray spectrometer operating independently
of the Mössbauer data accumulation in the following simultaneous
modes: NORMAL, COINCIDENCE and ANTI-COINCIDENCE (up to 3840 useable
channels in each mode) 4. The γ-ray spectrometer's Gauss
five-pole filter provides four, software-selectable (0.5 to 5
microseconds) shaping times constants 5. Downloadable transducer
reference function having 8192 points per full cycle with 12-bit
resolution 6. Transducer repetition frequency variable from
about 0.3 to about 90 Hz in small steps 7. Velocity window
settable in small steps from about 0.5 to about 150 mm/s 8.
Built-in laser based Michelson-Morley interferometer for precision
velocity calibration 9. Precision transducer being able to cover
velocity windows from about 0.5 to about 150 mm/s and equipped with
the positioning sensor; a transducer has a hollow central tube
allowing to work with the synchrotron radiation beams or to mount a
movable corner-prism velocity calibrator just back to the source;
the average source position could be set precisely 10. Two
ready-to-use nuclear detector heads having software-controlled
internal high voltage supplies, i.e., NaI(Tl) scintillation detector
head and Kr-filled proportional detector head - both detectors
having iron-free Be-windows 11. The Euro-bin back plane consists
of: short lines for individual block-to-block connections, parallel
and serial buses, power supplies and a few unused long lines so any
new, specialized block may be easily inserted into one of three
remaining slots. Analogue signal can be fed from one of the
nuclear heads or from the external source like the solid-state
detector. Input circuit for the latter case is ready to accept
signals from the optically coupled preamplifiers. Multi-scalar
signal is fed internally to the bank #1, while the bank #2 could be
used to either accumulate laser calibration data or external pulses.
All functions are controlled via developed software. Optical
calibration system has advanced design allowing to calibrate low and
high velocities with high accuracy. It is insensitive to the
acoustical noise.
Innovative Aspects: The system is
easily expandable and allows for straightforward data processing.
One can accumulate Mössbauer spectra up to 2047 points per spectrum
with highly linear velocity scale. Unusual reference functions are
easily generated and tested for the harmonics content. Velocity
calibration is an easy and straightforward task due to the intrinsic
optical calibration system. Round-corner reference functions can be
optimised to assure the best performance of the transducer. All four
spectra (two Mössbauer and Gamma coincidence/anticoincidence) are
accumulated simultaneously and independently.
Main
Advantages: Flexibility of design and operation; remote control
and ability to store and recall parameters used in previous runs
makes the spectrometer ideal for routine industrial applications. On
the other hand, the spectrometer meets all the quality standards
required for advanced basic research like, e.g. Mössbauer holography
or synchrotron radiation nuclear interferometry. The transducer has
a hollow central tube. |
| Technology Keywords: |
|
| Current Stage of Development: |
Already on the market |
| Exploitation of RTD Results: |
None |
| Intellectual Property Rights: |
Secret know-how
|
| Comments |
No special rights. |
| Organisation/Company Type: |
Other Private research & service
SME |
| Organisation/Company Size: |
<50 |
| Brief Market Application Codes: |
- Chemical industry
- Heavy metals industry, smelting
- Materials technology
- Measurement methods
- Pharmaceutical/Comestics
- Waste management
- BIOLOGICAL SCIENCES
- Environment protection
- OTHERS (Specify in Market Application Highlights)
Comments
|
| Detailed Market Application Codes
(VEIC): |
Keywords
- Other Medical/Health Related
Highlights Mössbauer spectrometers could be used
as non-destructive analytical tools in materials research and
testing, biology, medicine, and environmental monitoring. |
| Collaboration Type: |
- Commercial Agreement with Technical Assistance
- Financial resources
Comments The company
is looking for a partner from the medicine or metrology branch for
co-operation. Technical Assistance in implementation of technology
is a necessary part of the agreement. |
| Preferred Countries for diffusion: |
ALL |
| Additional
Information: |
|
| Contact Name: |
Kubik |
| Contact First name: |
Artur |
| Phone: |
+48 12 628 28 45 |
| Fax: |
+48 12 632 47 95 |
| Email: |
mailto:akubik@transfer.edu.pl |